Crystal and molecular structure of 17α-acetoxy-21-hydroxy-1,4-pregnadiene-3,20-dione
The title compound 17α‐acetoxy‐21‐hydroxy‐1,4‐pregnadiene‐3,20‐dione crystallizes in the orthorhombic space group P 212121 with four molecules in the unit cell and the lattice parameters a = 10.950, b = 11.857, c = 15.634 Å. The crystal structure was determined by direct methods and refined by full...
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| Veröffentlicht in: | Crystal research and technology (1979) 1990-02, Vol.25 (2), p.151-156 |
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| container_title | Crystal research and technology (1979) |
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| creator | Scharfenberg-Pfeiffer, D. Megges, R. Bohl, M. Simon, K. Stopsack, H. |
| description | The title compound 17α‐acetoxy‐21‐hydroxy‐1,4‐pregnadiene‐3,20‐dione crystallizes in the orthorhombic space group P 212121 with four molecules in the unit cell and the lattice parameters a = 10.950, b = 11.857, c = 15.634 Å. The crystal structure was determined by direct methods and refined by full matrix least squares calculations up to the discrepancy factor R = 0.050.
Die Titelverbindung 17α‐Acetoxy‐21‐hydroxy‐1,4‐pregnadien‐3,20‐dion kristallisiert in der orthorhombischen Raumgruppe P 212121 mit vier Molekülen in der Elementarzelle und den Gitterkonstanten a = 10,950, b = 11,857, c = 15,634 Å. Die Kristallstruktur wurde mit direkten Methoden bestimmt und mit der Methode der kleinsten Quadrate bis zu einem R‐Wert von 0,050 verfeinert. |
| doi_str_mv | 10.1002/crat.2170250210 |
| format | Article |
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Die Titelverbindung 17α‐Acetoxy‐21‐hydroxy‐1,4‐pregnadien‐3,20‐dion kristallisiert in der orthorhombischen Raumgruppe P 212121 mit vier Molekülen in der Elementarzelle und den Gitterkonstanten a = 10,950, b = 11,857, c = 15,634 Å. Die Kristallstruktur wurde mit direkten Methoden bestimmt und mit der Methode der kleinsten Quadrate bis zu einem R‐Wert von 0,050 verfeinert.</description><identifier>ISSN: 0232-1300</identifier><identifier>EISSN: 1521-4079</identifier><identifier>DOI: 10.1002/crat.2170250210</identifier><identifier>CODEN: CRTEDF</identifier><language>eng</language><publisher>Berlin: WILEY-VCH Verlag</publisher><subject>Aliphatic, non-condensed and condensed benzenic, and alicyclic compounds ; Condensed matter: structure, mechanical and thermal properties ; Exact sciences and technology ; Organic compounds ; Physics ; Structure of solids and liquids; crystallography ; Structure of specific crystalline solids</subject><ispartof>Crystal research and technology (1979), 1990-02, Vol.25 (2), p.151-156</ispartof><rights>Copyright © 1990 WILEY‐VCH Verlag GmbH & Co. KGaA</rights><rights>1993 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c3600-9c8619392122b18f3c5d044d76652ff600190b73eb9a8e77b379af8a6b168e233</citedby><cites>FETCH-LOGICAL-c3600-9c8619392122b18f3c5d044d76652ff600190b73eb9a8e77b379af8a6b168e233</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fcrat.2170250210$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fcrat.2170250210$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,780,784,1416,27923,27924,45573,45574</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=4548581$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Scharfenberg-Pfeiffer, D.</creatorcontrib><creatorcontrib>Megges, R.</creatorcontrib><creatorcontrib>Bohl, M.</creatorcontrib><creatorcontrib>Simon, K.</creatorcontrib><creatorcontrib>Stopsack, H.</creatorcontrib><title>Crystal and molecular structure of 17α-acetoxy-21-hydroxy-1,4-pregnadiene-3,20-dione</title><title>Crystal research and technology (1979)</title><addtitle>Cryst. Res. Technol</addtitle><description>The title compound 17α‐acetoxy‐21‐hydroxy‐1,4‐pregnadiene‐3,20‐dione crystallizes in the orthorhombic space group P 212121 with four molecules in the unit cell and the lattice parameters a = 10.950, b = 11.857, c = 15.634 Å. The crystal structure was determined by direct methods and refined by full matrix least squares calculations up to the discrepancy factor R = 0.050.
Die Titelverbindung 17α‐Acetoxy‐21‐hydroxy‐1,4‐pregnadien‐3,20‐dion kristallisiert in der orthorhombischen Raumgruppe P 212121 mit vier Molekülen in der Elementarzelle und den Gitterkonstanten a = 10,950, b = 11,857, c = 15,634 Å. Die Kristallstruktur wurde mit direkten Methoden bestimmt und mit der Methode der kleinsten Quadrate bis zu einem R‐Wert von 0,050 verfeinert.</description><subject>Aliphatic, non-condensed and condensed benzenic, and alicyclic compounds</subject><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Exact sciences and technology</subject><subject>Organic compounds</subject><subject>Physics</subject><subject>Structure of solids and liquids; crystallography</subject><subject>Structure of specific crystalline solids</subject><issn>0232-1300</issn><issn>1521-4079</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>1990</creationdate><recordtype>article</recordtype><recordid>eNqFkLFOwzAURS0EEqUws2ZgrNtnO4ljMZUAAamAhFp1tBzHgUCaVHYqms_iR_gmUgUVMTG9O5xzn3QROicwJgB0oq1qxpRwoAFQAgdoQAJKsA9cHKIBUEYxYQDH6MS5NwAQoU8HaBHb1jWq9FSVeau6NHpTKuu5xm50s7HGq3OP8K9PrLRp6m2Lu8rXNrO7SEY-XlvzUqmsMJXBbEQBZ0VdmVN0lKvSmbOfO0SL25t5fIdnT8l9PJ1hzUIALHQUEsEEJZSmJMqZDjLw_YyHYUDzvEOIgJQzkwoVGc5TxoXKIxWmJIwMZWyIJn2vtrVz1uRybYuVsq0kIHeryN0q8neVzrjojbVyWpW5VZUu3F7zAz8KItJhlz32UZSm_a9Vxs_T-Z8nuLcL15jt3lb2XYac8UAuHxMpkuQ6WT7M5RX7BlOngYU</recordid><startdate>199002</startdate><enddate>199002</enddate><creator>Scharfenberg-Pfeiffer, D.</creator><creator>Megges, R.</creator><creator>Bohl, M.</creator><creator>Simon, K.</creator><creator>Stopsack, H.</creator><general>WILEY-VCH Verlag</general><general>WILEY‐VCH Verlag</general><general>Wiley-VCH</general><scope>BSCLL</scope><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>199002</creationdate><title>Crystal and molecular structure of 17α-acetoxy-21-hydroxy-1,4-pregnadiene-3,20-dione</title><author>Scharfenberg-Pfeiffer, D. ; Megges, R. ; Bohl, M. ; Simon, K. ; Stopsack, H.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3600-9c8619392122b18f3c5d044d76652ff600190b73eb9a8e77b379af8a6b168e233</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>1990</creationdate><topic>Aliphatic, non-condensed and condensed benzenic, and alicyclic compounds</topic><topic>Condensed matter: structure, mechanical and thermal properties</topic><topic>Exact sciences and technology</topic><topic>Organic compounds</topic><topic>Physics</topic><topic>Structure of solids and liquids; crystallography</topic><topic>Structure of specific crystalline solids</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Scharfenberg-Pfeiffer, D.</creatorcontrib><creatorcontrib>Megges, R.</creatorcontrib><creatorcontrib>Bohl, M.</creatorcontrib><creatorcontrib>Simon, K.</creatorcontrib><creatorcontrib>Stopsack, H.</creatorcontrib><collection>Istex</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><jtitle>Crystal research and technology (1979)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Scharfenberg-Pfeiffer, D.</au><au>Megges, R.</au><au>Bohl, M.</au><au>Simon, K.</au><au>Stopsack, H.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Crystal and molecular structure of 17α-acetoxy-21-hydroxy-1,4-pregnadiene-3,20-dione</atitle><jtitle>Crystal research and technology (1979)</jtitle><addtitle>Cryst. Res. Technol</addtitle><date>1990-02</date><risdate>1990</risdate><volume>25</volume><issue>2</issue><spage>151</spage><epage>156</epage><pages>151-156</pages><issn>0232-1300</issn><eissn>1521-4079</eissn><coden>CRTEDF</coden><abstract>The title compound 17α‐acetoxy‐21‐hydroxy‐1,4‐pregnadiene‐3,20‐dione crystallizes in the orthorhombic space group P 212121 with four molecules in the unit cell and the lattice parameters a = 10.950, b = 11.857, c = 15.634 Å. The crystal structure was determined by direct methods and refined by full matrix least squares calculations up to the discrepancy factor R = 0.050.
Die Titelverbindung 17α‐Acetoxy‐21‐hydroxy‐1,4‐pregnadien‐3,20‐dion kristallisiert in der orthorhombischen Raumgruppe P 212121 mit vier Molekülen in der Elementarzelle und den Gitterkonstanten a = 10,950, b = 11,857, c = 15,634 Å. Die Kristallstruktur wurde mit direkten Methoden bestimmt und mit der Methode der kleinsten Quadrate bis zu einem R‐Wert von 0,050 verfeinert.</abstract><cop>Berlin</cop><pub>WILEY-VCH Verlag</pub><doi>10.1002/crat.2170250210</doi><tpages>6</tpages></addata></record> |
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| ispartof | Crystal research and technology (1979), 1990-02, Vol.25 (2), p.151-156 |
| issn | 0232-1300 1521-4079 |
| language | eng |
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| source | Wiley Online Library |
| subjects | Aliphatic, non-condensed and condensed benzenic, and alicyclic compounds Condensed matter: structure, mechanical and thermal properties Exact sciences and technology Organic compounds Physics Structure of solids and liquids crystallography Structure of specific crystalline solids |
| title | Crystal and molecular structure of 17α-acetoxy-21-hydroxy-1,4-pregnadiene-3,20-dione |
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