Design and synthesis of γ‐Fe 2 O 3 @Ag‐S‐CH 2 ‐COOH nanocatalyst for one‐pot synthesis of 2,3‐dihydroquinazolin‐4(1 H )‐ones and their anti‐skin cancer activity
The ongoing work describes the catalytic evaluation of γ‐Fe 2 O 3 @Ag‐S‐CH 2 ‐COOH magnetic nanoparticles utilizing γ‐Fe 2 O 3 obtained from waste iron rust for one‐pot synthesis of 2,3‐dihydroquinazolin‐4(1 H )‐ones. As‐prepared γ‐Fe 2 O 3 @Ag‐S‐CH 2 ‐COOH nanoparticles were characterized by Fourie...
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| Veröffentlicht in: | Applied organometallic chemistry 2023-06, Vol.37 (6) |
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| container_title | Applied organometallic chemistry |
| container_volume | 37 |
| creator | Gurav, Akshay Pandurang Gurav, Rutikesh Pandit Zond, Rutuja Ramesh Satyanarayan, Nayak Devappa Belur, Nippu Ningegowda Hangirgekar, Shankar Poshatti |
| description | The ongoing work describes the catalytic evaluation of γ‐Fe
2
O
3
@Ag‐S‐CH
2
‐COOH magnetic nanoparticles utilizing γ‐Fe
2
O
3
obtained from waste iron rust for one‐pot synthesis of 2,3‐dihydroquinazolin‐4(1
H
)‐ones. As‐prepared γ‐Fe
2
O
3
@Ag‐S‐CH
2
‐COOH nanoparticles were characterized by Fourier transform infrared spectroscopy (FT‐IR), X‐ray diffraction (XRD), scanning electron microscopy (SEM), energy‐dispersive X‐ray spectroscopy (EDX), dynamic light scattering (DLS), transmission electron microscopy (TEM), X‐ray photoelectron spectroscopy (XPS), and Brunauer–Emmett–Teller (BET) technique. The catalytic performance of greener γ‐Fe
2
O
3
@Ag‐S‐CH
2
‐COOH nanoparticles was utilized in the synthesis of 2,3‐dihydroquinazolin‐4(1
H
)‐ones. The excellent catalytic performance was shown by magnetic nanoparticles in addition to its ease of separation by an external magnet and can be recycled for five consecutive turns without significant loss of catalytic activity. Furthermore, the synthesized 2,3‐dihydroquinazolin‐4(1
H
)‐ones were confirmed by FT‐IR,
1
H,
13
C nuclear magnetic resonance (NMR), and mass spectrometry. Moreover, the synthesized 2,3‐dihydroquinazolin‐4(1
H
)‐ones were evaluated for their anticancer efficiency against the human skin cancer cell line B16F10 along with molecular docking investigation. |
| doi_str_mv | 10.1002/aoc.7086 |
| format | Article |
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2
O
3
@Ag‐S‐CH
2
‐COOH magnetic nanoparticles utilizing γ‐Fe
2
O
3
obtained from waste iron rust for one‐pot synthesis of 2,3‐dihydroquinazolin‐4(1
H
)‐ones. As‐prepared γ‐Fe
2
O
3
@Ag‐S‐CH
2
‐COOH nanoparticles were characterized by Fourier transform infrared spectroscopy (FT‐IR), X‐ray diffraction (XRD), scanning electron microscopy (SEM), energy‐dispersive X‐ray spectroscopy (EDX), dynamic light scattering (DLS), transmission electron microscopy (TEM), X‐ray photoelectron spectroscopy (XPS), and Brunauer–Emmett–Teller (BET) technique. The catalytic performance of greener γ‐Fe
2
O
3
@Ag‐S‐CH
2
‐COOH nanoparticles was utilized in the synthesis of 2,3‐dihydroquinazolin‐4(1
H
)‐ones. The excellent catalytic performance was shown by magnetic nanoparticles in addition to its ease of separation by an external magnet and can be recycled for five consecutive turns without significant loss of catalytic activity. Furthermore, the synthesized 2,3‐dihydroquinazolin‐4(1
H
)‐ones were confirmed by FT‐IR,
1
H,
13
C nuclear magnetic resonance (NMR), and mass spectrometry. Moreover, the synthesized 2,3‐dihydroquinazolin‐4(1
H
)‐ones were evaluated for their anticancer efficiency against the human skin cancer cell line B16F10 along with molecular docking investigation.</description><identifier>ISSN: 0268-2605</identifier><identifier>EISSN: 1099-0739</identifier><identifier>DOI: 10.1002/aoc.7086</identifier><language>eng</language><ispartof>Applied organometallic chemistry, 2023-06, Vol.37 (6)</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-crossref_primary_10_1002_aoc_70863</cites><orcidid>0000-0002-0985-3742 ; 0000-0003-3723-8509 ; 0000-0003-4511-3749 ; 0000-0002-6182-9328 ; 0000-0002-3360-050X ; 0000-0002-1047-8839</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids></links><search><creatorcontrib>Gurav, Akshay Pandurang</creatorcontrib><creatorcontrib>Gurav, Rutikesh Pandit</creatorcontrib><creatorcontrib>Zond, Rutuja Ramesh</creatorcontrib><creatorcontrib>Satyanarayan, Nayak Devappa</creatorcontrib><creatorcontrib>Belur, Nippu Ningegowda</creatorcontrib><creatorcontrib>Hangirgekar, Shankar Poshatti</creatorcontrib><title>Design and synthesis of γ‐Fe 2 O 3 @Ag‐S‐CH 2 ‐COOH nanocatalyst for one‐pot synthesis of 2,3‐dihydroquinazolin‐4(1 H )‐ones and their anti‐skin cancer activity</title><title>Applied organometallic chemistry</title><description>The ongoing work describes the catalytic evaluation of γ‐Fe
2
O
3
@Ag‐S‐CH
2
‐COOH magnetic nanoparticles utilizing γ‐Fe
2
O
3
obtained from waste iron rust for one‐pot synthesis of 2,3‐dihydroquinazolin‐4(1
H
)‐ones. As‐prepared γ‐Fe
2
O
3
@Ag‐S‐CH
2
‐COOH nanoparticles were characterized by Fourier transform infrared spectroscopy (FT‐IR), X‐ray diffraction (XRD), scanning electron microscopy (SEM), energy‐dispersive X‐ray spectroscopy (EDX), dynamic light scattering (DLS), transmission electron microscopy (TEM), X‐ray photoelectron spectroscopy (XPS), and Brunauer–Emmett–Teller (BET) technique. The catalytic performance of greener γ‐Fe
2
O
3
@Ag‐S‐CH
2
‐COOH nanoparticles was utilized in the synthesis of 2,3‐dihydroquinazolin‐4(1
H
)‐ones. The excellent catalytic performance was shown by magnetic nanoparticles in addition to its ease of separation by an external magnet and can be recycled for five consecutive turns without significant loss of catalytic activity. Furthermore, the synthesized 2,3‐dihydroquinazolin‐4(1
H
)‐ones were confirmed by FT‐IR,
1
H,
13
C nuclear magnetic resonance (NMR), and mass spectrometry. Moreover, the synthesized 2,3‐dihydroquinazolin‐4(1
H
)‐ones were evaluated for their anticancer efficiency against the human skin cancer cell line B16F10 along with molecular docking investigation.</description><issn>0268-2605</issn><issn>1099-0739</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><recordid>eNqVkE1Ow0AMhUcIJMKPxBG8LBIpnqSkzQ7UUmWXBeyj0WTSDoSZMh6QwoojcJfeg0NwElzEhiULy_ZnP8t6QpxJHEvE7FJ5PZ7irNgTicSyTHGal_siwayYpVmBV4fiiOgBEctCThKxXRiyKwfKtUCDi2tuCXwHn9uv94-lgQxqyOH6ZsXtHce8YrTLdV2BU85rFVU_UITOB_DO8Gzj499j2UXOuLXroQ3--cU69eZ765hNRhIqOOeKpfTzBsts4CpapvRoHWjltGGko321cTgRB53qyZz-5mMxWt7ez6tUB08UTNdsgn1SYWgkNjtTGjal2ZmS_2P1G7V4cXs</recordid><startdate>202306</startdate><enddate>202306</enddate><creator>Gurav, Akshay Pandurang</creator><creator>Gurav, Rutikesh Pandit</creator><creator>Zond, Rutuja Ramesh</creator><creator>Satyanarayan, Nayak Devappa</creator><creator>Belur, Nippu Ningegowda</creator><creator>Hangirgekar, Shankar Poshatti</creator><scope>AAYXX</scope><scope>CITATION</scope><orcidid>https://orcid.org/0000-0002-0985-3742</orcidid><orcidid>https://orcid.org/0000-0003-3723-8509</orcidid><orcidid>https://orcid.org/0000-0003-4511-3749</orcidid><orcidid>https://orcid.org/0000-0002-6182-9328</orcidid><orcidid>https://orcid.org/0000-0002-3360-050X</orcidid><orcidid>https://orcid.org/0000-0002-1047-8839</orcidid></search><sort><creationdate>202306</creationdate><title>Design and synthesis of γ‐Fe 2 O 3 @Ag‐S‐CH 2 ‐COOH nanocatalyst for one‐pot synthesis of 2,3‐dihydroquinazolin‐4(1 H )‐ones and their anti‐skin cancer activity</title><author>Gurav, Akshay Pandurang ; Gurav, Rutikesh Pandit ; Zond, Rutuja Ramesh ; Satyanarayan, Nayak Devappa ; Belur, Nippu Ningegowda ; Hangirgekar, Shankar Poshatti</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-crossref_primary_10_1002_aoc_70863</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Gurav, Akshay Pandurang</creatorcontrib><creatorcontrib>Gurav, Rutikesh Pandit</creatorcontrib><creatorcontrib>Zond, Rutuja Ramesh</creatorcontrib><creatorcontrib>Satyanarayan, Nayak Devappa</creatorcontrib><creatorcontrib>Belur, Nippu Ningegowda</creatorcontrib><creatorcontrib>Hangirgekar, Shankar Poshatti</creatorcontrib><collection>CrossRef</collection><jtitle>Applied organometallic chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Gurav, Akshay Pandurang</au><au>Gurav, Rutikesh Pandit</au><au>Zond, Rutuja Ramesh</au><au>Satyanarayan, Nayak Devappa</au><au>Belur, Nippu Ningegowda</au><au>Hangirgekar, Shankar Poshatti</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Design and synthesis of γ‐Fe 2 O 3 @Ag‐S‐CH 2 ‐COOH nanocatalyst for one‐pot synthesis of 2,3‐dihydroquinazolin‐4(1 H )‐ones and their anti‐skin cancer activity</atitle><jtitle>Applied organometallic chemistry</jtitle><date>2023-06</date><risdate>2023</risdate><volume>37</volume><issue>6</issue><issn>0268-2605</issn><eissn>1099-0739</eissn><abstract>The ongoing work describes the catalytic evaluation of γ‐Fe
2
O
3
@Ag‐S‐CH
2
‐COOH magnetic nanoparticles utilizing γ‐Fe
2
O
3
obtained from waste iron rust for one‐pot synthesis of 2,3‐dihydroquinazolin‐4(1
H
)‐ones. As‐prepared γ‐Fe
2
O
3
@Ag‐S‐CH
2
‐COOH nanoparticles were characterized by Fourier transform infrared spectroscopy (FT‐IR), X‐ray diffraction (XRD), scanning electron microscopy (SEM), energy‐dispersive X‐ray spectroscopy (EDX), dynamic light scattering (DLS), transmission electron microscopy (TEM), X‐ray photoelectron spectroscopy (XPS), and Brunauer–Emmett–Teller (BET) technique. The catalytic performance of greener γ‐Fe
2
O
3
@Ag‐S‐CH
2
‐COOH nanoparticles was utilized in the synthesis of 2,3‐dihydroquinazolin‐4(1
H
)‐ones. The excellent catalytic performance was shown by magnetic nanoparticles in addition to its ease of separation by an external magnet and can be recycled for five consecutive turns without significant loss of catalytic activity. Furthermore, the synthesized 2,3‐dihydroquinazolin‐4(1
H
)‐ones were confirmed by FT‐IR,
1
H,
13
C nuclear magnetic resonance (NMR), and mass spectrometry. Moreover, the synthesized 2,3‐dihydroquinazolin‐4(1
H
)‐ones were evaluated for their anticancer efficiency against the human skin cancer cell line B16F10 along with molecular docking investigation.</abstract><doi>10.1002/aoc.7086</doi><orcidid>https://orcid.org/0000-0002-0985-3742</orcidid><orcidid>https://orcid.org/0000-0003-3723-8509</orcidid><orcidid>https://orcid.org/0000-0003-4511-3749</orcidid><orcidid>https://orcid.org/0000-0002-6182-9328</orcidid><orcidid>https://orcid.org/0000-0002-3360-050X</orcidid><orcidid>https://orcid.org/0000-0002-1047-8839</orcidid></addata></record> |
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| issn | 0268-2605 1099-0739 |
| language | eng |
| recordid | cdi_crossref_primary_10_1002_aoc_7086 |
| source | Wiley Journals |
| title | Design and synthesis of γ‐Fe 2 O 3 @Ag‐S‐CH 2 ‐COOH nanocatalyst for one‐pot synthesis of 2,3‐dihydroquinazolin‐4(1 H )‐ones and their anti‐skin cancer activity |
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