Fabrication of multilayer Nb_2O_5 nanoporous film by anodization of niobium foils
Multilayer Nb2O5 nanoporous films were successfully synthesized on Nb surfaces by the control anodization process in ethylene glycol containing 4 vol% HF and 2 vol% H2O2 electrolyte. The nanoporous films are characterized in detail by field-emission scanning electron microscopy（FESEM）, transmission...
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| creator | Guang-Zhong Li Hui-Ping Tang Wen-Yan Zhang Gang Li Lan-Lan Yu Ya-Ning Li |
| description | Multilayer Nb2O5 nanoporous films were successfully synthesized on Nb surfaces by the control anodization process in ethylene glycol containing 4 vol% HF and 2 vol% H2O2 electrolyte. The nanoporous films are characterized in detail by field-emission scanning electron microscopy（FESEM）, transmission electron microscopy（TEM）, and X-ray diffraction（XRD）. The Nb_2O_5 nanoporous films have a multilayer morphology with the side wall thickness of ～5 nm, irregular pores with a diameter of ～25 nm, and a length of up to 7.39 lm, depending on the anodization time. A mechanism for the multilayer Nb2O5 nanoporous formation was also discussed. These nanoporous materials can be very useful in the fields of solar cells, gas sensors, catalysts, optical filters, and capacitors. |
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The nanoporous films are characterized in detail by field-emission scanning electron microscopy（FESEM）, transmission electron microscopy（TEM）, and X-ray diffraction（XRD）. The Nb_2O_5 nanoporous films have a multilayer morphology with the side wall thickness of ～5 nm, irregular pores with a diameter of ～25 nm, and a length of up to 7.39 lm, depending on the anodization time. A mechanism for the multilayer Nb2O5 nanoporous formation was also discussed. 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| ispartof | 稀有金属：英文版, 2015 (2), p.77-80 |
| issn | 1001-0521 1867-7185 |
| language | eng |
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| source | Springer Nature - Complete Springer Journals; Alma/SFX Local Collection |
| subjects | Nb2O5 制造 扫描电子显微镜 纳米多孔材料 纳米多孔膜 透射电子显微镜 阳极化 阳极氧化工艺 |
| title | Fabrication of multilayer Nb_2O_5 nanoporous film by anodization of niobium foils |
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