Determination of Gallic Acid by Flow Injection Analysis Based on LuminoI-AgNO3-Ag NPs Chemiluminescence System
A novel flow injection procedure has been developed for the determination of gallic acid based on the en- hancement function for luminol-AgNO3-Ag NPs chemiluminescence (CL) system by gallic acid. The enhancement mechanism was proposed for the reinforcing effect of the gallic acid on the CL system. T...
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Veröffentlicht in: | 中国化学:英文版 2012, Vol.30 (4), p.837-841 |
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creator | 李世凤 孙惠敏 王东 钱莉 朱燕 陶善军 |
description | A novel flow injection procedure has been developed for the determination of gallic acid based on the en- hancement function for luminol-AgNO3-Ag NPs chemiluminescence (CL) system by gallic acid. The enhancement mechanism was proposed for the reinforcing effect of the gallic acid on the CL system. The UV-vis absorption spectrum and CL emission spectrum were applied to confirm the mechanism. The method is simple, rapid and sen- sitive with a detection limit of 5 × 10^-10 g.mL-l and a linear range of 8.0 × 10^-10- 1.0 × 10-7 g.mL-1. The relative standard deviation (RSD) is 1.3% for eleven measurements of 5 × 10^-8 g-mL-1 gallic acid. The method has been successfully applied to the determination of gallic acid in Chinese proprietary medicine--Jianmin Yanhou tablets and synthesized samples. |
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The enhancement mechanism was proposed for the reinforcing effect of the gallic acid on the CL system. The UV-vis absorption spectrum and CL emission spectrum were applied to confirm the mechanism. The method is simple, rapid and sen- sitive with a detection limit of 5 × 10^-10 g.mL-l and a linear range of 8.0 × 10^-10- 1.0 × 10-7 g.mL-1. The relative standard deviation (RSD) is 1.3% for eleven measurements of 5 × 10^-8 g-mL-1 gallic acid. The method has been successfully applied to the determination of gallic acid in Chinese proprietary medicine--Jianmin Yanhou tablets and synthesized samples.</description><identifier>ISSN: 1001-604X</identifier><identifier>EISSN: 1614-7065</identifier><language>eng</language><subject>UV-Vis吸收光谱 ; 化学发光体系 ; 没食子酸 ; 流动注射分析法 ; 测定 ; 相对标准偏差 ; 硝酸银 ; 银纳米粒子</subject><ispartof>中国化学:英文版, 2012, Vol.30 (4), p.837-841</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Uhttp://image.cqvip.com/vip1000/qk/84126X/84126X.jpg</thumbnail><link.rule.ids>314,780,784,4024</link.rule.ids></links><search><creatorcontrib>李世凤 孙惠敏 王东 钱莉 朱燕 陶善军</creatorcontrib><title>Determination of Gallic Acid by Flow Injection Analysis Based on LuminoI-AgNO3-Ag NPs Chemiluminescence System</title><title>中国化学:英文版</title><addtitle>Chinese Journal of Chemistry</addtitle><description>A novel flow injection procedure has been developed for the determination of gallic acid based on the en- hancement function for luminol-AgNO3-Ag NPs chemiluminescence (CL) system by gallic acid. 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The enhancement mechanism was proposed for the reinforcing effect of the gallic acid on the CL system. The UV-vis absorption spectrum and CL emission spectrum were applied to confirm the mechanism. The method is simple, rapid and sen- sitive with a detection limit of 5 × 10^-10 g.mL-l and a linear range of 8.0 × 10^-10- 1.0 × 10-7 g.mL-1. The relative standard deviation (RSD) is 1.3% for eleven measurements of 5 × 10^-8 g-mL-1 gallic acid. The method has been successfully applied to the determination of gallic acid in Chinese proprietary medicine--Jianmin Yanhou tablets and synthesized samples.</abstract></addata></record> |
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subjects | UV-Vis吸收光谱 化学发光体系 没食子酸 流动注射分析法 测定 相对标准偏差 硝酸银 银纳米粒子 |
title | Determination of Gallic Acid by Flow Injection Analysis Based on LuminoI-AgNO3-Ag NPs Chemiluminescence System |
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