Sulfonated Carbon Catalyzed Biginelli Reaction for One-Pot Synthesis of 3,4-Dihydropyrimidin-2（1H）-ones and-thiones

Sulfonated Carbon Catalyzed Biginelli Reaction for One-Pot Synthesis of 3,4-Dihydropyrimidin-2（1H）-ones and-thiones

A sulfonated carbon material was shown to be a highly efficient,eco-friendly,and recyclable solid acid catalyst for the Biginelli reaction of β-ketoester,aldehyde,and urea or thiourea under solvent-free conditions.It gave 3,4-dihydropyrimidin-2（1H）-ones and-thiones in good to excellent yields.This m...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:催化学报 2012, Vol.33 (4), p.706-710
1. Verfasser: Maryam MOGHADDAS Abolghasem DAVOODNIA Majid M. HERAVI Niloofar TAVAKOLI-HOSEINI
Format: Artikel
Sprache:chi
Schlagworte:
催化
化学
高压
高温
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
container_end_page 710
container_issue 4
container_start_page 706
container_title 催化学报
container_volume 33
creator Maryam MOGHADDAS Abolghasem DAVOODNIA Majid M. HERAVI Niloofar TAVAKOLI-HOSEINI
description A sulfonated carbon material was shown to be a highly efficient,eco-friendly,and recyclable solid acid catalyst for the Biginelli reaction of β-ketoester,aldehyde,and urea or thiourea under solvent-free conditions.It gave 3,4-dihydropyrimidin-2（1H）-ones and-thiones in good to excellent yields.This method has the advantages of a simple procedure with easy work-up,short reaction time,and high yields.The catalyst can be recycled after a simple work-up and was reused four times without substantial reduction in activity.
format Article
fullrecord <record><control><sourceid>chongqing</sourceid><recordid>TN_cdi_chongqing_primary_41738406</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><cqvip_id>41738406</cqvip_id><sourcerecordid>41738406</sourcerecordid><originalsourceid>FETCH-chongqing_primary_417384063</originalsourceid><addsrcrecordid>eNqNjF2KwjAUhYPMgGV0D5l3A2lSbefVP3xTRt8l2rS9kLnRJCJxBbon9-QWrOAC5uk7nO9wOiRJi1wwwUf5B0m4GEr2U8i8S_rew45zIYaFzERCzuuTqSyqoEs6UW5nsUVQJl7aYgw1oDYG6K9W-wCtrKyjS9RsZQNdRwyN9uCpragcZGwKTSydPUQHf1ACMvG4X9PF435jFrWnCksWGnjlHvmslPG6_-YX-Z7PNpMF2zcW6yNgvT20L8rFbZbmssj4SP5n8wRMIU-K</addsrcrecordid><sourcetype>Publisher</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype></control><display><type>article</type><title>Sulfonated Carbon Catalyzed Biginelli Reaction for One-Pot Synthesis of 3,4-Dihydropyrimidin-2（1H）-ones and-thiones</title><source>Access via ScienceDirect (Elsevier)</source><creator>Maryam MOGHADDAS Abolghasem DAVOODNIA Majid M. HERAVI Niloofar TAVAKOLI-HOSEINI</creator><creatorcontrib>Maryam MOGHADDAS Abolghasem DAVOODNIA Majid M. HERAVI Niloofar TAVAKOLI-HOSEINI</creatorcontrib><description>A sulfonated carbon material was shown to be a highly efficient,eco-friendly,and recyclable solid acid catalyst for the Biginelli reaction of β-ketoester,aldehyde,and urea or thiourea under solvent-free conditions.It gave 3,4-dihydropyrimidin-2（1H）-ones and-thiones in good to excellent yields.This method has the advantages of a simple procedure with easy work-up,short reaction time,and high yields.The catalyst can be recycled after a simple work-up and was reused four times without substantial reduction in activity.</description><identifier>ISSN: 0253-9837</identifier><identifier>EISSN: 1872-2067</identifier><language>chi</language><subject>催化 ; 化学 ; 高压 ; 高温</subject><ispartof>催化学报, 2012, Vol.33 (4), p.706-710</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Uhttp://image.cqvip.com/vip1000/qk/93027X/93027X.jpg</thumbnail><link.rule.ids>314,780,784,4024</link.rule.ids></links><search><creatorcontrib>Maryam MOGHADDAS Abolghasem DAVOODNIA Majid M. HERAVI Niloofar TAVAKOLI-HOSEINI</creatorcontrib><title>Sulfonated Carbon Catalyzed Biginelli Reaction for One-Pot Synthesis of 3,4-Dihydropyrimidin-2（1H）-ones and-thiones</title><title>催化学报</title><addtitle>Chinese Journal of Catalysis</addtitle><description>A sulfonated carbon material was shown to be a highly efficient,eco-friendly,and recyclable solid acid catalyst for the Biginelli reaction of β-ketoester,aldehyde,and urea or thiourea under solvent-free conditions.It gave 3,4-dihydropyrimidin-2（1H）-ones and-thiones in good to excellent yields.This method has the advantages of a simple procedure with easy work-up,short reaction time,and high yields.The catalyst can be recycled after a simple work-up and was reused four times without substantial reduction in activity.</description><subject>催化</subject><subject>化学</subject><subject>高压</subject><subject>高温</subject><issn>0253-9837</issn><issn>1872-2067</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><recordid>eNqNjF2KwjAUhYPMgGV0D5l3A2lSbefVP3xTRt8l2rS9kLnRJCJxBbon9-QWrOAC5uk7nO9wOiRJi1wwwUf5B0m4GEr2U8i8S_rew45zIYaFzERCzuuTqSyqoEs6UW5nsUVQJl7aYgw1oDYG6K9W-wCtrKyjS9RsZQNdRwyN9uCpragcZGwKTSydPUQHf1ACMvG4X9PF435jFrWnCksWGnjlHvmslPG6_-YX-Z7PNpMF2zcW6yNgvT20L8rFbZbmssj4SP5n8wRMIU-K</recordid><startdate>2012</startdate><enddate>2012</enddate><creator>Maryam MOGHADDAS Abolghasem DAVOODNIA Majid M. HERAVI Niloofar TAVAKOLI-HOSEINI</creator><scope>2RA</scope><scope>92L</scope><scope>CQIGP</scope><scope>~WA</scope></search><sort><creationdate>2012</creationdate><title>Sulfonated Carbon Catalyzed Biginelli Reaction for One-Pot Synthesis of 3,4-Dihydropyrimidin-2（1H）-ones and-thiones</title><author>Maryam MOGHADDAS Abolghasem DAVOODNIA Majid M. HERAVI Niloofar TAVAKOLI-HOSEINI</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-chongqing_primary_417384063</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>chi</language><creationdate>2012</creationdate><topic>催化</topic><topic>化学</topic><topic>高压</topic><topic>高温</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Maryam MOGHADDAS Abolghasem DAVOODNIA Majid M. HERAVI Niloofar TAVAKOLI-HOSEINI</creatorcontrib><collection>中文科技期刊数据库</collection><collection>中文科技期刊数据库-CALIS站点</collection><collection>中文科技期刊数据库-7.0平台</collection><collection>中文科技期刊数据库- 镜像站点</collection><jtitle>催化学报</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Maryam MOGHADDAS Abolghasem DAVOODNIA Majid M. HERAVI Niloofar TAVAKOLI-HOSEINI</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Sulfonated Carbon Catalyzed Biginelli Reaction for One-Pot Synthesis of 3,4-Dihydropyrimidin-2（1H）-ones and-thiones</atitle><jtitle>催化学报</jtitle><addtitle>Chinese Journal of Catalysis</addtitle><date>2012</date><risdate>2012</risdate><volume>33</volume><issue>4</issue><spage>706</spage><epage>710</epage><pages>706-710</pages><issn>0253-9837</issn><eissn>1872-2067</eissn><abstract>A sulfonated carbon material was shown to be a highly efficient,eco-friendly,and recyclable solid acid catalyst for the Biginelli reaction of β-ketoester,aldehyde,and urea or thiourea under solvent-free conditions.It gave 3,4-dihydropyrimidin-2（1H）-ones and-thiones in good to excellent yields.This method has the advantages of a simple procedure with easy work-up,short reaction time,and high yields.The catalyst can be recycled after a simple work-up and was reused four times without substantial reduction in activity.</abstract></addata></record>
fulltext fulltext
identifier ISSN: 0253-9837
ispartof 催化学报, 2012, Vol.33 (4), p.706-710
issn 0253-9837
1872-2067
language chi
recordid cdi_chongqing_primary_41738406
source Access via ScienceDirect (Elsevier)
subjects 催化
化学
高压
高温
title Sulfonated Carbon Catalyzed Biginelli Reaction for One-Pot Synthesis of 3,4-Dihydropyrimidin-2（1H）-ones and-thiones
url https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2024-12-24T23%3A39%3A15IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-chongqing&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Sulfonated%20Carbon%20Catalyzed%20Biginelli%20Reaction%20for%20One-Pot%20Synthesis%20of%203,4-Dihydropyrimidin-2%EF%BC%881H%EF%BC%89-ones%20and-thiones&rft.jtitle=%E5%82%AC%E5%8C%96%E5%AD%A6%E6%8A%A5&rft.au=Maryam%20MOGHADDAS%20Abolghasem%20DAVOODNIA%20Majid%20M.%20HERAVI%20Niloofar%20TAVAKOLI-HOSEINI&rft.date=2012&rft.volume=33&rft.issue=4&rft.spage=706&rft.epage=710&rft.pages=706-710&rft.issn=0253-9837&rft.eissn=1872-2067&rft_id=info:doi/&rft_dat=%3Cchongqing%3E41738406%3C/chongqing%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_id=info:pmid/&rft_cqvip_id=41738406&rfr_iscdi=true