A single-solenoid pulsed-magnet system for single-crystal scattering studies
We present a pulsed-magnet system that enables x-ray single-crystal diffraction in addition to powder and spectroscopic studies with the magnetic field applied on or close to the scattering plane. The apparatus consists of a single large-bore solenoid, cooled by liquid nitrogen. A second independent...
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| creator | Islam, Zahirul Capatina, Dana Ruff, Jacob P C Das, Ritesh K Trakhtenberg, Emil Nojiri, Hiroyuki Narumi, Yasuo Welp, Ulrich Canfield, Paul C |
| description | We present a pulsed-magnet system that enables x-ray single-crystal diffraction in addition to powder and spectroscopic studies with the magnetic field applied on or close to the scattering plane. The apparatus consists of a single large-bore solenoid, cooled by liquid nitrogen. A second independent closed-cycle cryostat is used for cooling samples near liquid helium temperatures. Pulsed magnetic fields close to \(\sim 30\) T with a zero-to-peak-field rise time of \(\sim\)2.9 ms are generated by discharging a 40 kJ capacitor bank into the magnet coil. The unique characteristic of this instrument is the preservation of maximum scattering angle (\(\sim 23.6^\circ\)) on the entrance and exit sides of the magnet bore by virtue of a novel double-funnel insert. This instrument will facilitate x-ray diffraction and spectroscopic studies that are impractical, if not impossible, to perform using split-pair and narrow-opening solenoid magnets, and offers a practical solution for preserving optical access in future higher-field pulsed magnets. |
| doi_str_mv | 10.48550/arxiv.1109.6713 |
| format | Article |
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The apparatus consists of a single large-bore solenoid, cooled by liquid nitrogen. A second independent closed-cycle cryostat is used for cooling samples near liquid helium temperatures. Pulsed magnetic fields close to \(\sim 30\) T with a zero-to-peak-field rise time of \(\sim\)2.9 ms are generated by discharging a 40 kJ capacitor bank into the magnet coil. The unique characteristic of this instrument is the preservation of maximum scattering angle (\(\sim 23.6^\circ\)) on the entrance and exit sides of the magnet bore by virtue of a novel double-funnel insert. 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This instrument will facilitate x-ray diffraction and spectroscopic studies that are impractical, if not impossible, to perform using split-pair and narrow-opening solenoid magnets, and offers a practical solution for preserving optical access in future higher-field pulsed magnets.</description><subject>Capacitor banks</subject><subject>Entrances</subject><subject>Helium</subject><subject>Liquid helium</subject><subject>Liquid nitrogen</subject><subject>Magnet coils</subject><subject>Magnetic fields</subject><subject>Magnets</subject><subject>Physics - Instrumentation and Detectors</subject><subject>Physics - Strongly Correlated Electrons</subject><subject>Scattering angle</subject><subject>Single crystals</subject><subject>Spectroscopic analysis</subject><subject>X-ray diffraction</subject><issn>2331-8422</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GOX</sourceid><recordid>eNo1j8tqwzAQRUWh0JBm31UxdC1XmvFY8jKEvsDQTfZGtuXg4FcluTR_X6dpVhcuZ4Z7GHuQIk40kXg27qf9jqUUWZwqiTdsBYiS6wTgjm28PwohIFVAhCuWbyPfDofOcj92dhjbOprmztua9-Yw2BD5kw-2j5rRXcHKLZXpIl-ZEKxbysiHuW6tv2e3jVmON_-5ZvvXl_3uneefbx-7bc4NSeJZiUakVZqJpAJJGUJqUSqZyqopSZVJQpbI6BLQalK1ynSlEqXrhlChAFyzx8vbP9Nicm1v3Kk4Gxdn4wV4ugCTG79m60NxHGc3LJMKEBoAMlKEv0HGWEI</recordid><startdate>20120207</startdate><enddate>20120207</enddate><creator>Islam, Zahirul</creator><creator>Capatina, Dana</creator><creator>Ruff, Jacob P C</creator><creator>Das, Ritesh K</creator><creator>Trakhtenberg, Emil</creator><creator>Nojiri, Hiroyuki</creator><creator>Narumi, Yasuo</creator><creator>Welp, Ulrich</creator><creator>Canfield, Paul C</creator><general>Cornell University Library, arXiv.org</general><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>L6V</scope><scope>M7S</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope><scope>GOX</scope></search><sort><creationdate>20120207</creationdate><title>A single-solenoid pulsed-magnet system for single-crystal scattering studies</title><author>Islam, Zahirul ; 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The apparatus consists of a single large-bore solenoid, cooled by liquid nitrogen. A second independent closed-cycle cryostat is used for cooling samples near liquid helium temperatures. Pulsed magnetic fields close to \(\sim 30\) T with a zero-to-peak-field rise time of \(\sim\)2.9 ms are generated by discharging a 40 kJ capacitor bank into the magnet coil. The unique characteristic of this instrument is the preservation of maximum scattering angle (\(\sim 23.6^\circ\)) on the entrance and exit sides of the magnet bore by virtue of a novel double-funnel insert. This instrument will facilitate x-ray diffraction and spectroscopic studies that are impractical, if not impossible, to perform using split-pair and narrow-opening solenoid magnets, and offers a practical solution for preserving optical access in future higher-field pulsed magnets.</abstract><cop>Ithaca</cop><pub>Cornell University Library, arXiv.org</pub><doi>10.48550/arxiv.1109.6713</doi><oa>free_for_read</oa></addata></record> |
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| subjects | Capacitor banks Entrances Helium Liquid helium Liquid nitrogen Magnet coils Magnetic fields Magnets Physics - Instrumentation and Detectors Physics - Strongly Correlated Electrons Scattering angle Single crystals Spectroscopic analysis X-ray diffraction |
| title | A single-solenoid pulsed-magnet system for single-crystal scattering studies |
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